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Synthesis:

12 ton Hydraulic Press (Carver)
0.4 L Benchtop Mini High Energy Ball Mill (MSE Supplies)
Thermolyne Benchtop Muffle Furnace (<1200 C; Thermo Scientific)
Lindberg Blue Mini-Mite Tube Furnace (<1100 C; Thermo Scientific)
Arc-melter furnace (<250 A current; Miller, Ames Lab US DOE)
Carbolite Gero Furnace (30-300 C) (Verder Scientific)
LabStar Pro SP 4-glove glovebox (MBraun)

Analysis and Characterization:

MetPrep 3 Semi-automatic Grinder Polisher (AlliedHighTech)
TrimSaw 2x Manual Table Diamond Saw (AlliedHighTech)
VH1102 Vickers Hardness Microindenter (Buehler)
Axioscope Microscopy Station (500x max; Zeiss)

  • Photochemical Reactor 500 mL, 450 W lamp (Ace Glass)
  • Quartz Ampoule Sealing Station